Lab 5: Atomic Emission Spectrometry by Inductively Coupled Plasma (ICP)

Equipment:

Perkin-Elmer Optima 7000DV ICP optical emission spectrometer (OES) with a CCDarray detector and a cyclonic spray chamber & concentric nebulizer for liquids. The ICP includes a Perkin-Elmer S10 autosampler and peristaltic pump for sample input under computer control for automated measurements.

Handouts:

None

References:

• D.A. Skoog, F.J. Holler & S.R. Crouch, Principles of Instrumental Analysis, 6^th ed, 2007:
  • Chap 8: An introduction to optical atomic spectrometry
  • Chap 10: Atomic emission spectrometry
• D.C. Harris, Quantitative Chemical Analysis, 8^th ed, 2011:
  • Chap 4: Statistics
  • Chap 5: Calibration methods
  • Chap 20: Atomic spectroscopy
• NIST Handbook of Basic Atomic Spectroscopic Data website

Lab description:

Get a PDF of

• The lab experiment
• Instructions for using the ICP-OES
• Codes for using the ICP-OES PC

Last modified April 05 2011 11:38 AM